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https://scidar.kg.ac.rs/handle/123456789/10514
Title: | Effect of milling and annealing on microstructural, electrical and magnetic properties of electrodeposited Ni-11.3fe-1.4W alloy |
Authors: | Ribic-Zelenovic, Lenka ![]() ![]() Spasojević M. Ćirović N. ![]() Spasojević P. Maricic, Aleksa ![]() ![]() |
Issue Date: | 2012 |
Abstract: | A nanostructured Ni-11.3Fe-1.4W alloy deposit was obtained from an ammonium citrate bath at a current density of 600 mAcm -2. XRD analysis shows that the deposit contains an amorphous matrix having embedded nanocrystals of the FCC phase of the solid solution of Fe and W in Ni with the average crystal grain size of 8.8 nm. The deposit has a high internal microstrain value and a high minimum density of chaotically distributed dislocations. The effect of milling and annealing of the Ni-11.3Fe-1.4W alloy on electrical and magnetic properties was studied. Structural changes in the alloy take place during both annealing and milling. Upon deposition, the alloy was heated to 420 °C. Heating resulted in structural relaxation which induced a decrease in electrical resistivity and an increase in magnetic permeability of the alloy. Further heating of the alloy at temperatures higher than 420 °C led to crystallization which caused a reduction in both electrical resistivity and magnetic permeability. The milling of the alloy for up to 12 hours caused a certain degree of structural relaxation and crystallization of the alloy. The increase in crystal grain size up to 11 nm and the partial structural relaxation induced a decrease in electrical resistivity and an increase in magnetic permeability of the alloy. Heating the powders obtained by milling at 420 °C led to complete structural relaxation, reduced electrical resistivity, and increased magnetic permeability. During heating of the powders obtained by milling at temperatures above 420 °C, crystallization and a significant increase in crystal grain size occurred, leading to a reduction in both electrical resistivity and magnetic permeability. The best magnetic properties were exhibited by the alloys milled for 12 hours and annealed thereafter at 420 °C. In these alloys, crystal grains were found to have an optimum size, and complete relaxation took place, resulting in a maximum increase in magnetic permeability. |
URI: | https://scidar.kg.ac.rs/handle/123456789/10514 |
Type: | article |
DOI: | 10.2298/SOS1202197S |
ISSN: | 0350-820X |
SCOPUS: | 2-s2.0-84866384876 |
Appears in Collections: | Faculty of Agronomy, Čačak |
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