Please use this identifier to cite or link to this item: https://scidar.kg.ac.rs/handle/123456789/11255
Title: Synthesis, structural and electrochemical characterization of novel 1,3-ketoureas bearing a ferrocenyl group
Authors: Minić, Aleksandra
Bugarinović, Jovana
Bogdanovic, Goran A.
Pejović, Anka
Radulovic, Niko
Damljanović, Ivan
Stevanović, Dragana
Issue Date: 2018
Abstract: © 2017 Elsevier Ltd Twenty-two novel 1,3-ketourea derivatives bearing ferrocene moiety were synthesized in good-to-excellent yields (up to 99%) via simple and efficient protocol. This solvent- and catalyst-free synthesis was achieved by additions of different ferrocene-containing Mannich bases – 3-(arylamino)-1-ferrocenylpropan-1-ones to phenyl isocyanate promoted only by ultrasound irradiations at ambient temperature. All synthesized 1-aryl-3-phenyl-1-(3-ferrocenyl-3-oxopropyl)ureas were characterized by standard spectral data (1H NMR, 13C NMR and IR), and their electrochemical behavior were investigated by cyclic voltammetry. Detailed single-crystal X-ray diffraction analysis of three representative ferrocene-containing 1,3-ketoureas, among which one crystallized with two independent molecules in an asymmetric unit, were done.
URI: https://scidar.kg.ac.rs/handle/123456789/11255
Type: article
DOI: 10.1016/j.poly.2017.12.018
ISSN: 0277-5387
SCOPUS: 2-s2.0-85039944060
Appears in Collections:Faculty of Science, Kragujevac

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