Please use this identifier to cite or link to this item: https://scidar.kg.ac.rs/handle/123456789/13293
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dc.rights.licenseopenAccess-
dc.contributor.authorBjelović, Ljiljana-
dc.contributor.authorGlišić, Biljana-
dc.contributor.authorŽivković, Marija-
dc.contributor.authorKanjevac, Tatjana-
dc.date.accessioned2021-06-15T07:42:24Z-
dc.date.available2021-06-15T07:42:24Z-
dc.date.issued2019-
dc.identifier.citationBjelović, L. Z., Glišić, B. Đ., Živković, M. D., & Kanjevac, T. V. [2019]. Investigation of p-chloroaniline formation in the reactions between different endodontic irrigants. Kragujevac Journal of Science, (41), 43-52.en_US
dc.identifier.issn1450-9636en_US
dc.identifier.urihttps://scidar.kg.ac.rs/handle/123456789/13293-
dc.description.abstractThe aim of this study was to determine whether p-chloroaniline (PCA) is formed in the reactions of sodium hypochlorite (NaOCl) with final rinse chlorhexidine (CHX), QMix (combination of ethylenediaminetetraacetic acid (EDTA), CHX and detergent) and EDTA/CHX solutions by thin-layer chromatography (TLC), proton nuclear magnetic resonance (1H NMR) and infrared (IR) spectroscopy. Commercially available 5.25% NaOCl solution was mixed with 2% CHX and QMix in 1:1 (v/v) ratio at room temperature. Furthermore, 2% CHX was associated with 17% EDTA under the same experimental conditions. The obtained solutions were evaluated qualitatively for color changing, precipitate and/or bubble formation and analyzed by TLC chromatography. The association products were investigated by spectroscopic (1H NMR and IR) methods in order to determine whether they contain PCA. It was found that interactions between NaOCl/CHX and CHX/EDTA led to forming of brown and white precipitate. When NaOCl was mixed with QMix, an orange-brown precipitate was formed. PCA was not detected as a product of the reactions between NaOCl and final rinse solutions of CHX, QMix and EDTA/CHX association.en_US
dc.language.isoenen_US
dc.publisherKragujevac Journal of Scienceen_US
dc.rightsinfo:eu-repo/semantics/openAccess-
dc.rights.urihttps://creativecommons.org/licenses/by-nc-nd/4.0/-
dc.sourceKragujevac Journal of Scienceen_US
dc.subjectp-Chloroanilineen_US
dc.subjectInfrared spectroscopyen_US
dc.subjectIrrigantsen_US
dc.subjectProton nuclear magnetic resonanceen_US
dc.subjectThin-layer chromatographyen_US
dc.titleInvestigation of p-chloroaniline formation in the reactions between different endodontic irrigantsen_US
dc.typearticleen_US
dc.description.versionPublisheden_US
dc.identifier.doi10.5937/KgJSci1941043Ben_US
dc.type.versionPublishedVersionen_US
Appears in Collections:Faculty of Science, Kragujevac

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