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Title: Synthesis of novel ferrocene-containing 1,3-thiazinan-2-imines: One-pot reaction promoted by ultrasound irradiation
Authors: Minić, Aleksandra
Bugarinović, Jovana
Pejović, Anka
Ilić Komatina D.
Bogdanovic, Goran A.
Damljanović, Ivan
Stevanović, Dragana
Journal: Tetrahedron Letters
Issue Date: 19-Sep-2018
Abstract: © 2018 Elsevier Ltd A simple one-pot synthesis of new ferrocene-containing 1,3-thiazinan-2-imines from 3-arylamino-1-ferrocenylpropan-1-ols and phenyl isothiocyanate has been developed. The key intermediate β-hydroxy thioureas were generated in situ using ultrasound irradiation and subsequent cyclization was achieved by the addition of acetic acid. The scope of the reaction towards various 3-arylamino-1-ferrocenylpropan-1-ols has been explored and the corresponding 3-aryl-6-ferrocenyl-N-phenyl-1,3-thiazinan-2-imines were obtained in moderate to high yields (52–90%).
Type: article
DOI: 10.1016/j.tetlet.2018.08.029
ISSN: 00404039
SCOPUS: 85051752405
Appears in Collections:Faculty of Science, Kragujevac

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